Handbook of Nanophase and Nanostructured Materials Vol. 2 : by Zhong Lin Wang

By Zhong Lin Wang

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MRS Bull.. December. 17–23 (1999) 28 2. 1 Major Components of a Transmission Electron Microscope A modern TEM is schematically shown in Fig. 1. It is composed of an illumination system, a specimen stage, an objective lens system, the magnification system, the data recording system(s), and the chemical analysis system. The electron gun typically uses an LaB6 thermionic emission source or a field emission source. The LaB6 gun gives a high illumination current, but the current density and the beam coherence are not as high as those of a field emission source.

Nanodiffraction, on the other hand, can work comfortably for thicker specimens as long as the image of the interface is visible. 27 shows the interface between a nanostructured TiN film and steel and the corresponding nanodiffraction patterns. The epitaxy is found to be steel ( ) 111 // TiN ( ) 011 . 27 Epitaxial growth of TiN on tool steel. (a) TEM bright-field image. The interface is indicated by an arrowhead. (b, c, d) Nanodiffraction patterns recorded from the tool steel, the interface and the TiN, respectively.

Cambridge University Press, Cambridge, United Kindom. 171–194 (1978) Stassis, C.. Methods of Experimental Physics. Vol. 23A, Neutron Scattering. , H. Wipf, K. H. Anderson, and H. Hahn. Phys. Rev. Lett.. , H. Wipf, T. J. Udovic, J. Weiβmüller, and H. Gleiter. J. : Condens. Matter. 7, 219 (1995) Todd, R. , M. A. M. Bourke, C. E. Borsa, R. J. Brook. Acta Meter.. , C. R. Hubbard, K. B. Alexander, P. F. Becher, J. A. Fernandez-Baca, and S. Spooner. J. Am. Ceram. Soc.. 77, 1569–1575 (1994) Wertheim, G.

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